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Beilstein J. Org. Chem. 2015, 11, 860–868, doi:10.3762/bjoc.11.96
Graphical Abstract
Figure 1: Molecular structures of tetrathiafulvalenes 1, bis-pyrrolotetrathiafulvalenes 2 and monopyrrolotetr...
Scheme 1: The two synthetic approaches used for the preparation of arylated monopyrrolotetrathiafulvalenes 1.
Scheme 2: Synthesis of arylated monopyrrolotetrathiafulvalenes 4a–f.
Figure 2: Copper(I) ligands 9a and 9b.
Figure 3: UV–vis spectra of compounds 4a,c–f (CH2Cl2, c = 4 × 10−5 M).
Figure 4: Cyclic voltammograms of compounds 4a,c [22] and 4d–f (plotted vs SCE; CH2Cl2/0.1 M Bu4NClO4).
Figure 5: Crystal packing of 4a viewed along the a axis and showing one layer of molecules. Short S···S conta...
Figure 6: Crystal packing of 4b showing a group of four molecules interconnected by multiple weak hydrogen bo...
Figure 7: Crystal packing of 4d viewed along the b axis. Molecules of 4d form layers parallel to the (001) pl...
Figure 8: Crystal packing of 4e showing a group of four molecules interconnected by multiple weak hydrogen bo...